(Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine

Base Information

• Chemical Name: (Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine
• CAS No.: 85322-34-5
• Molecular Formula: C₁₈H₁₇N₃O₂
• Molecular Weight: 307.352

Synonyms:(Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine

Chemical Property of (Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine

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Technology Process of (Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine

There total 1 articles about (Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.8%

p-methyl-γ-bromoacetoacetanilide (23976-42-3) + N-hydroxybenzenecarboximidamide (613-92-3) → (Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine (85322-34-5)

Guidance literature:

With toluene-4-sulfonic acid; In acetonitrile; for 3h; Heating;

Reference yield: 22.0%

(Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine (85322-34-5) → 2-phenyl-4-(p-tolylcarbamoyl)methyloxazole (99141-51-2) + Z-2-phenyl-4-(p-tolylcarbamoyl)methylene-2-oxazoline (99258-97-6) + E-2-phenyl-4-(p-tolylcarbamoyl)methylene-2-oxazoline (99141-48-7)

Guidance literature:

With hydrogen; nickel; In tetrahydrofuran; for 24h; under 760 Torr; Ambient temperature;

Reference yield: 20.0%

(Z)-5-(p-methylphenylcarbamoyl)-methylene-3-phenyl-5,6-dihydro-4H-1,2,4-oxadiazine (85322-34-5) → 2-phenyl-4-(p-tolylcarbamoyl)methyloxazole (99141-51-2) + 6-Hydroxymethyl-2-phenyl-4-pyrimidinone (84445-99-8) + Z-2-phenyl-4-(p-tolylcarbamoyl)methylene-2-oxazoline (99258-97-6) + E-2-phenyl-4-(p-tolylcarbamoyl)methylene-2-oxazoline (99141-48-7)

Guidance literature:

With hydrogen; nickel; In tetrahydrofuran; for 3h; under 2280 Torr; Ambient temperature;

upstream raw materials:

p-methyl-γ-bromoacetoacetanilide

N-hydroxybenzenecarboximidamide

Downstream raw materials:

N-(p-Tolyl)-3-hydroxybutanamide

N-(1-p-tolylcarbamoyl-2-propylidene)benzamide oxime

5,6-Dihydro-3-phenyl-5-(p-tolylcarbamoyl)methyl-4H-1,2,4-oxadiazine

2-phenyl-4-(p-tolylcarbamoyl)methyloxazole

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