1-benzyloxy-3-benzyloxycarbonylthiourea

Base Information

• Chemical Name: 1-benzyloxy-3-benzyloxycarbonylthiourea
• CAS No.: 187972-12-9
• Molecular Formula: C₁₆H₁₆N₂O₃S
• Molecular Weight: 316.381
• Mol file: 187972-12-9.mol

Synonyms:1-benzyloxy-3-benzyloxycarbonylthiourea

Chemical Property of 1-benzyloxy-3-benzyloxycarbonylthiourea

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzyloxy-3-benzyloxycarbonylthiourea

There total 2 articles about 1-benzyloxy-3-benzyloxycarbonylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → 1-benzyloxy-3-benzyloxycarbonylthiourea (187972-12-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dibenzo-18-crown-6 / benzene / 3 h / Heating

2: benzene

With dibenzo-18-crown-6; In benzene;

DOI:10.1080/00397919708005034

Reference yield:

N-benzyloxyamine (622-33-3) + benzyloxycarbonyl isothiocyanate (63220-36-0) → 1-benzyloxy-3-benzyloxycarbonylthiourea (187972-12-9)

Guidance literature:

In benzene; Yield given;

DOI:10.1080/00397919708005034

Reference yield: 87.0%

1-benzyloxy-3-benzyloxycarbonylthiourea (187972-12-9) + (4R,5R)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxan-5-ylamine → C39H47N3O6Si (272106-56-6)

Guidance literature:

With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1021/jo9915574

upstream raw materials:

N-benzyloxyamine

benzyloxycarbonyl isothiocyanate

benzyl chloroformate

Downstream raw materials:

C₃₉H₄₇N₃O₆Si

C₂₃H₂₉N₃O₆

((4aR,8R,8aS)-7-Benzyloxy-8-hydroxy-2,2-dimethyl-4a,7,8,8a-tetrahydro-4H-1,3-dioxa-5,7-diaza-naphthalen-6-yl)-carbamic acid benzyl ester

((4aR,8R,8aS)-7-Benzyloxy-2,2-dimethyl-8-triethylsilanyloxy-4a,7,8,8a-tetrahydro-4H-1,3-dioxa-5,7-diaza-naphthalen-6-yl)-carbamic acid benzyl ester