(2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

Base Information

Chemical Name:(2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide
CAS No.:500767-21-5
Molecular Formula:C₃₁H₃₇N₃O₆
Molecular Weight:547.651
Hs Code.:

Synonyms:(2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

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Chemical Property of (2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

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Technology Process of (2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

There total 3 articles about (2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 500767-14-6
(2S,5S,6S)-3-aza-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

: 500767-21-5
(2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm020951i

Reference yield:

: 6485-52-5
L-phenylglycine amide

: 500767-21-5
(2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / propan-2-ol / Heating

2: 85 percent / aq. K₂CO₃ / tetrahydrofuran / 20 °C

With potassium carbonate; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1021/jm020951i

Reference yield:

: 98760-08-8
(2R,3S)-3-[N-(tert-butyloxycarbonyl)amino]-1,2-epoxy-4-phenylbutane

: 500767-21-5
(2S,5S,6S)-3-aza-3-(benzyloxycarbonyl)-6-[(tert-butyloxycarbonyl)amino]-5-hydroxy-2,7-diphenylheptanoyl amide

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / propan-2-ol / Heating

2: 85 percent / aq. K₂CO₃ / tetrahydrofuran / 20 °C

With potassium carbonate; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1021/jm020951i