[2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II)

Base Information

• Chemical Name: [2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II)
• CAS No.: 1412456-51-9
• Molecular Formula: C₄₈H₃₆CuN₆O₆
• Molecular Weight: 856.396

Synonyms:[2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II)

Chemical Property of [2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II)

Chemical Property:

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Technology Process of [2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II)

There total 2 articles about [2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[2-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II) (95212-95-6) → [2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II) (1412456-51-9)

Guidance literature:

With N,N,N-trimethylhydrazinium iodide; potassium hydroxide; In dimethyl sulfoxide; at 75 ℃; for 0.75h; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.09.024

Reference yield:

[5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II) (95215-03-5) → [2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II) (1412456-51-9)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid / chloroform

2: N,N,N-trimethylhydrazinium iodide; potassium hydroxide / dimethyl sulfoxide / 0.75 h / 75 °C / Inert atmosphere

With nitric acid; N,N,N-trimethylhydrazinium iodide; potassium hydroxide; In chloroform; dimethyl sulfoxide;

DOI:10.1016/j.tetlet.2012.09.024

Reference yield: 88.0%

[2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II) (1412456-51-9) → 2-amino-3-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrin

Guidance literature:

With sulfuric acid; trifluoroacetic acid; In chloroform; at 20 ℃;

DOI:10.1016/j.tetlet.2012.09.024

upstream raw materials:

[2-nitro-5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II)

[5,10,15,20-tetrakis(3-methoxyphenyl)porphyrinato]copper(II)

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