(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

Base Information

Chemical Name:(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide
CAS No.:1402050-28-5
Molecular Formula:C₃₄H₅₅NOSSi
Molecular Weight:553.968
Hs Code.:

Synonyms:(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

Suppliers and Price of (S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

Chemical Property:

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Technology Process of (S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

There total 2 articles about (S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1402050-26-3
(S)-3-hydroxy-N,N,14-trimethylpentadecanethioamide

: 92886-86-7
tert-butyldiphenylsilyl triflate

: 1402050-28-5
(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jo301803h DOI:10.1021/jo301803h

Reference yield:

: 75853-49-5
12-methyltridecan-1-al

: 1402050-28-5
(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

With 2,6-dimethylpyridine; 2,2,5,7,8-pentamethylchroman-6-ol; mesitylcopper(I); (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo301803h DOI:10.1021/jo301803h