C₃₀H₂₄BrNO₃

Base Information

Chemical Name:C₃₀H₂₄BrNO₃
CAS No.:1298044-29-7
Molecular Formula:C₃₀H₂₄BrNO₃
Molecular Weight:526.429
Hs Code.:

C<sub>30</sub>H<sub>24</sub>BrNO<sub>3</sub>

Synonyms:C₃₀H₂₄BrNO₃

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Chemical Property of C₃₀H₂₄BrNO₃

Chemical Property:

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Technology Process of C₃₀H₂₄BrNO₃

There total 10 articles about C₃₀H₂₄BrNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1298044-27-5
(1R)-1-(6-bromo-2-methoxyquinolin-3-yl)-2-(naphthalen-1-yl)-1-phenylpent-4-en-2-ol

: 1298044-29-7
C₃₀H₂₄BrNO₃

Guidance literature:: With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; In 1,4-dioxane; water; at 20 ℃; for 2h;
DOI:10.1002/ejoc.201001720

Reference yield:

: 1298044-13-9
ethyl (E)-3-(6-bromo-2-chloroquinolin-3-yl)acrylate

: 1298044-29-7
C₃₀H₂₄BrNO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 2 h / 0 - 20 °C

1.2: 4 h

2.1: methanol / 8 h / 80 °C

3.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.67 h / -20 °C / Molecular sieve

3.2: 4 h / -20 °C

4.1: copper(l) cyanide / tetrahydrofuran; diethyl ether / 1 h / -40 °C

4.2: 3 h / -40 °C

4.3: 3 h

5.1: / dichloromethane / 1 h / 0 - 20 °C

6.1: diethyl ether / 1 h / 0 °C

7.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C

8.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran / 0.17 h / 20 °C

8.2: 0.5 h

9.1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water / 2 h / 20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; sodium periodate; osmium(VIII) oxide; copper(I) bromide dimethylsulfide complex; L-(+)-diisopropyl tartrate; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; hexane; dichloromethane; water; 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation / 8.2: Barbier type reaction;
DOI:10.1002/ejoc.201001720

Reference yield:

: 1298044-17-3
(E)-3-(6-bromo-2-methoxyquinolin-3-yl)prop-2-en-1-ol

: 1298044-29-7
C₃₀H₂₄BrNO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.67 h / -20 °C / Molecular sieve

1.2: 4 h / -20 °C

2.1: copper(l) cyanide / tetrahydrofuran; diethyl ether / 1 h / -40 °C

2.2: 3 h / -40 °C

2.3: 3 h

3.1: / dichloromethane / 1 h / 0 - 20 °C

4.1: diethyl ether / 1 h / 0 °C

5.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C

6.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran / 0.17 h / 20 °C

6.2: 0.5 h

7.1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water / 2 h / 20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; sodium periodate; osmium(VIII) oxide; copper(I) bromide dimethylsulfide complex; L-(+)-diisopropyl tartrate; copper(l) cyanide; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; 1.1: Sharpless epoxidation / 1.2: Sharpless epoxidation / 6.2: Barbier type reaction;
DOI:10.1002/ejoc.201001720