N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide

Base Information

Chemical Name:N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide
CAS No.:1268375-12-7
Molecular Formula:C₅₄H₄₆N₂O₅
Molecular Weight:802.97
Hs Code.:

Synonyms:N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide

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Chemical Property of N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide

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Technology Process of N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide

There total 3 articles about N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.8%

: 869276-74-4
N,N’-di-(2,6-diisopropylphenyl)-1-bromoperylene-3,4:9,10-tetracarboxylic acid diimide

: 108-95-2,27073-41-2
phenol

: 1268375-12-7
N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide

Guidance literature:: With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.dyepig.2010.11.006

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1268375-12-7
N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; iodine / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 80 °C

1.3: 96 h / 120 °C

2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 24 h / 120 °C / Inert atmosphere

With sulfuric acid; iodine; potassium carbonate; In 1-methyl-pyrrolidin-2-one;
DOI:10.1016/j.dyepig.2010.11.006

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1268375-12-7
N,N'-bis(2,6-diisopropylphenyl)-1-phenoxy-perylene-3,4,9,10-tetracarboxydiimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; iodine / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 80 °C

1.3: 96 h / 120 °C

2.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 24 h / 120 °C / Inert atmosphere

With sulfuric acid; iodine; potassium carbonate; In 1-methyl-pyrrolidin-2-one;
DOI:10.1016/j.dyepig.2010.11.006