2-bromo-1-cyclohexenecarboxylic acid amide

Base Information

Chemical Name:2-bromo-1-cyclohexenecarboxylic acid amide
CAS No.:1010098-53-9
Molecular Formula:C₇H₁₀BrNO
Molecular Weight:204.066
Hs Code.:

Synonyms:2-bromo-1-cyclohexenecarboxylic acid amide

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Chemical Property of 2-bromo-1-cyclohexenecarboxylic acid amide

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Technology Process of 2-bromo-1-cyclohexenecarboxylic acid amide

There total 3 articles about 2-bromo-1-cyclohexenecarboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68965-62-8
2-bromocyclohex-1-enecarboxylic acid

: 1010098-53-9
2-bromo-1-cyclohexenecarboxylic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; DMF / CH₂Cl₂ / 4 h / 0 °C

2.1: 1,1,1,3,3,3-hexamethyl-disilazane / CH₂Cl₂ / 20 °C

2.2: 0.816 g / methanol / CH₂Cl₂ / 3 h / 20 °C

With oxalyl dichloride; N,N-dimethyl-formamide; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane;
DOI:10.1002/anie.200600111

Reference yield:

: 159389-47-6
2-bromo-1-cyclohexene-1-carbonyl chloride

: 1010098-53-9
2-bromo-1-cyclohexenecarboxylic acid amide

Guidance literature:: 2-bromo-1-cyclohexene-1-carbonyl chloride; With 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; at 20 ℃;

With methanol; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1002/anie.200600111

Reference yield:

: 38127-47-8
2-bromocyclohex-1-ene-1-carbaldehyde

: 1010098-53-9
2-bromo-1-cyclohexenecarboxylic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / aq. NaClO₂; aq. NaH₂PO₄; aq. H₂O₂ / acetonitrile / 2 h / 10 °C

2.1: oxalyl dichloride; DMF / CH₂Cl₂ / 4 h / 0 °C

3.1: 1,1,1,3,3,3-hexamethyl-disilazane / CH₂Cl₂ / 20 °C

3.2: 0.816 g / methanol / CH₂Cl₂ / 3 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; oxalyl dichloride; dihydrogen peroxide; N,N-dimethyl-formamide; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; acetonitrile;
DOI:10.1002/anie.200600111