2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

Base Information

Chemical Name:2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol
CAS No.:1026873-37-9
Molecular Formula:C₁₄H₂₈O₃
Molecular Weight:244.375
Hs Code.:

Synonyms:2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

Suppliers and Price of 2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

Chemical Property:

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Technology Process of 2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

There total 10 articles about 2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: tert-Butyl-[2-((1S,2R,3S,6R)-3-isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethoxy]-dimethyl-silane

: 1026873-37-9
2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1246/cl.1998.739

Reference yield:

: 2216-51-5
(-)-menthol

: 1026873-37-9
2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

Guidance literature:: Multi-step reaction with 10 steps

2: TsN₃, Et₃N

3: Rh₂(OAc)4

4: 1.) MeONa, 2.) p-TsOH / 1.) MeOH, 2.) CH₂Cl₂

5: 90 percent / LiAlH₄ / diethyl ether

6: 91 percent / imidazole / dimethylformamide

7: 83 percent / Dess-Martin periodinane / CH₂Cl₂

8: 89 percent / L-Selectride / tetrahydrofuran

9: 74 percent / Et₃N / CH₂Cl₂

10: 94 percent / TBAF / tetrahydrofuran

With 1H-imidazole; dirhodium tetraacetate; lithium aluminium tetrahydride; 4-toluenesulfonyl azide; tetrabutyl ammonium fluoride; sodium methylate; L-Selectride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/cl.1998.739

Reference yield:

: 127236-74-2
(1R,2S,5R)-(-)-menthyl diazoacetoacetate

: 1026873-37-9
2-((1S,2R,3S,6R)-3-Isopropyl-2-methoxymethoxy-6-methyl-cyclohexyl)-ethanol

Guidance literature:: Multi-step reaction with 8 steps

1: Rh₂(OAc)4

2: 1.) MeONa, 2.) p-TsOH / 1.) MeOH, 2.) CH₂Cl₂

3: 90 percent / LiAlH₄ / diethyl ether

4: 91 percent / imidazole / dimethylformamide

5: 83 percent / Dess-Martin periodinane / CH₂Cl₂

6: 89 percent / L-Selectride / tetrahydrofuran

7: 74 percent / Et₃N / CH₂Cl₂

8: 94 percent / TBAF / tetrahydrofuran

With 1H-imidazole; dirhodium tetraacetate; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; sodium methylate; L-Selectride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/cl.1998.739