2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol

Base Information

Chemical Name:2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol
CAS No.:1356339-52-0
Molecular Formula:C₂₆H₃₃N₅O₅
Molecular Weight:495.579
Hs Code.:

Synonyms:2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol

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Chemical Property of 2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol

Chemical Property:

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Technology Process of 2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol

There total 4 articles about 2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 62402-19-1
N-(2-methoxyethyl)-N-(pyridin-2-ylmethyl)amine

: 98437-49-1
1,3-bis(bromomethyl)-4-nitrophenol

: 1356339-52-0
2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c1dt11187f

Reference yield:

: 150975-29-4
2-methoxy-N-((pyridin-2-yl)methylene)ethanamine

: 1356339-52-0
2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0 °C

2: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c1dt11187f

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 1356339-52-0
2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-nitrophenol

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 0 - 20 °C

2: sodium tetrahydroborate / methanol / 0 °C

3: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c1dt11187f