Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid

Base Information

Chemical Name:Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid
CAS No.:74995-89-4
Molecular Formula:C₁₄H₁₈O₃S
Molecular Weight:266.361
Hs Code.:

Synonyms:Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid

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Chemical Property of Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid

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Technology Process of Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid

There total 9 articles about Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 74995-88-3
Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-thiophenyl-α-D-threo-hex-2-enopyranosid

: 74995-89-4
Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 5 ℃; for 0.5h;

Reference yield:

: 74995-84-9
methyl 4-O-benzoyl-6-bromo-2,6-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

: 74995-89-4
Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / Et₃N, H₂ / Raney-Ni / methanol / 2942.03 Torr

2: 85 percent / SOCl₂ / benzene; pyridine / 3 h / 5 °C

3: 98 percent / 2 N NaOH / ethanol / 15 h / Ambient temperature

4: 73 percent / tri-n-butylphosphane / benzene / 3 h

5: 77 percent / 85percent 3-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / 0 - 5 °C

With sodium hydroxide; thionyl chloride; tributylphosphine; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; nickel; In pyridine; methanol; ethanol; dichloromethane; benzene;

Reference yield:

: 6752-52-9,13264-07-8,18424-64-1,19231-32-4,77481-74-4,77481-75-5,77481-76-6,77481-77-7,78086-67-6,100100-70-7
Methyl-4,6-O-benzyliden-2-desoxy-3-C-methyl-α-D-ribo-hexopyranosid

: 74995-89-4
Methyl-2,3,4,6-tetradesoxy-3-C-methyl-4-(phenylsulfinyl)-α-D-threo-hex-2-enopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: N-bromosuccinimide, BaCO₃ / CCl₄ / 2 h / Heating

2: 83 percent / Et₃N, H₂ / Raney-Ni / methanol / 2942.03 Torr

3: 85 percent / SOCl₂ / benzene; pyridine / 3 h / 5 °C

4: 98 percent / 2 N NaOH / ethanol / 15 h / Ambient temperature

5: 73 percent / tri-n-butylphosphane / benzene / 3 h

6: 77 percent / 85percent 3-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / 0 - 5 °C

With sodium hydroxide; N-Bromosuccinimide; thionyl chloride; tributylphosphine; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; barium carbonate; nickel; In pyridine; methanol; tetrachloromethane; ethanol; dichloromethane; benzene;