Methyl-4,6-didesoxy-3-C-methyl-N-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid

Base Information

Chemical Name:Methyl-4,6-didesoxy-3-C-methyl-N-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid
CAS No.:78013-86-2
Molecular Formula:C₁₆H₂₅NO₆S
Molecular Weight:359.444
Hs Code.:

Synonyms:Methyl-4,6-didesoxy-3-C-methyl-N-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-4,6-didesoxy-3-C-methyl-N-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid

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Technology Process of Methyl-4,6-didesoxy-3-C-methyl-N-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid

There total 23 articles about Methyl-4,6-didesoxy-3-C-methyl-N-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 78013-85-1
Methyl-4,6-didesoxy-3-C-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid

: 74-88-4
methyl iodide

: 78013-86-2
Methyl-4,6-didesoxy-3-C-methyl-N-methyl-4-(p-tolylsulfonylamino)-α-D-altropyranosid

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 70 ℃; for 17h;

Reference yield:

: 82793-12-2
tert-Butyl-((2R,3R,6S)-2-methoxy-4,6-dimethyl-3,6-dihydro-2H-pyran-3-yloxy)-dimethyl-silane

: 78013-86-2,82793-15-5,82793-18-8
N-((2R,3R,4R,5S)-4,5-Dihydroxy-6-methoxy-2,4-dimethyl-tetrahydro-pyran-3-yl)-4,N-dimethyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / OsO₄ / 8 h / 60 °C / oxyamination reaction

2: 89 percent / tBuOK

4: HCl / methanol

With hydrogenchloride; potassium tert-butylate; osmium(VIII) oxide; In methanol;
DOI:10.1016/S0040-4039(00)86735-0

Reference yield:

: 82793-10-0
tert-Butyl-((2S,3S,4S,5R,6R)-2-methoxy-4,6-dimethyl-5-phenylselanyl-tetrahydro-pyran-3-yloxy)-dimethyl-silane

: 78013-86-2,82793-15-5,82793-18-8
N-((2R,3R,4R,5S)-4,5-Dihydroxy-6-methoxy-2,4-dimethyl-tetrahydro-pyran-3-yl)-4,N-dimethyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: NaIO₄

2: 70 percent / OsO₄ / 8 h / 60 °C / oxyamination reaction

3: 89 percent / tBuOK

5: HCl / methanol

With hydrogenchloride; sodium periodate; potassium tert-butylate; osmium(VIII) oxide; In methanol;
DOI:10.1016/S0040-4039(00)86735-0