3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride

Base Information

Chemical Name:3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride
CAS No.:1201663-82-2
Molecular Formula:C₂₇H₁₉Cl₃FNO₄S
Molecular Weight:578.876
Hs Code.:

Synonyms:3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride

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Chemical Property of 3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride

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Technology Process of 3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride

There total 7 articles about 3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1201663-80-0
3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoic acid

: 1201663-82-2
3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

Reference yield:

: 1172338-38-3
(4'-chlorobiphenyl-3-yl)methanamine hydrochloride

: 1201663-82-2
3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane; isopropyl alcohol / 1 h / 20 °C

1.2: 3 h / 20 °C / Inert atmosphere

1.3: 0.17 h

2.1: triethylamine / dichloromethane / 18.5 h / 20 °C / Inert atmosphere

2.2: 6 h / 40 °C

2.3: pH 1 - 2

3.1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; isopropyl alcohol;

Reference yield:

: 1201663-79-7
1-(4'-chlorobiphenyl-3-yl)-N-(4-fluorobenzyl)methanamine

: 1201663-82-2
3-chloro-5-(N-((4'-chlorobiphenyl-3-yl)methyl)-N-(4-fluorobenzyl)sulfamoyl)-4-hydroxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 18.5 h / 20 °C / Inert atmosphere

1.2: 6 h / 40 °C

1.3: pH 1 - 2

2.1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;