phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside
CAS No.:1287768-28-8
Molecular Formula:C₃₄H₃₀O₈S
Molecular Weight:598.673
Hs Code.:

Synonyms:phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

Suppliers and Price of phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

There total 4 articles about phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 138857-50-8
phenyl 2,3-bis-O-benzoyl-1-thio-β-D-glucopyranoside

: 1287768-28-8
phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide; at 50 ℃; for 1h;
DOI:10.1021/jo200076z

Reference yield:

: 71676-30-7,87508-18-7,138922-03-9,87508-17-6
(2R,4aR,6S,7R,8R,8aS)-2-Phenyl-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

: 1287768-28-8
phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C

2: toluene-4-sulfonic acid / methanol; dichloromethane / 8 h / 35 °C

3: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 1 h / 50 °C

With pyridine; camphor-10-sulfonic acid; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200076z

Reference yield:

: 98-88-4
benzoyl chloride

: 1287768-28-8
phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C

2: toluene-4-sulfonic acid / methanol; dichloromethane / 8 h / 35 °C

3: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 1 h / 50 °C

With pyridine; camphor-10-sulfonic acid; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200076z