C₇₂H₆₅N₆O₁₆PS

Base Information

Chemical Name:C₇₂H₆₅N₆O₁₆PS
CAS No.:106521-95-3
Molecular Formula:C₇₂H₆₅N₆O₁₆PS
Molecular Weight:1333.38
Hs Code.:

C<sub>72</sub>H<sub>65</sub>N<sub>6</sub>O<sub>16</sub>PS

Synonyms:C₇₂H₆₅N₆O₁₆PS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇₂H₆₅N₆O₁₆PS

Chemical Property:

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Technology Process of C₇₂H₆₅N₆O₁₆PS

There total 5 articles about C₇₂H₆₅N₆O₁₆PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 94189-81-8
3,3'-O,N-dibenzoylthymidine

: C₄₈H₄₄N₄O₉PS⁽¹⁺⁾*Cl^(1-)

: 106521-95-3
C₇₂H₆₅N₆O₁₆PS

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In pyridine; for 0.00833333h;
DOI:10.1021/jo00381a047

Reference yield:

: 94189-75-0
N³-benzoyl thymidine

: 106521-95-3
C₇₂H₆₅N₆O₁₆PS

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / dimethylformamide / 0.17 h

2: mesitylenedisulfonyl chloride (MDS) / 0.17 h

3: 100 percent / phosphinic acid (PSA), pyridine / 0.17 h

4: isodurenedisulfonyl chloride (DDS) / pyridine / 0.08 h

5: 100 percent / (i-Pr)2NEt / pyridine / 0.01 h

With pyridine; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; hypophosphorous acid; 2,4,5,6-tetramethylbenzenedisulfonyl dichloride; N-ethyl-N,N-diisopropylamine; In pyridine; N,N-dimethyl-formamide;
DOI:10.1021/jo00381a047

Reference yield:

: 106502-50-5
3-Benzoyl-1-{(2R,4S,5R)-4-hydroxy-5-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-2-yl}-5-methyl-1H-pyrimidine-2,4-dione

: 106521-95-3
C₇₂H₆₅N₆O₁₆PS

Guidance literature:: Multi-step reaction with 4 steps

1: mesitylenedisulfonyl chloride (MDS) / 0.17 h

2: 100 percent / phosphinic acid (PSA), pyridine / 0.17 h

3: isodurenedisulfonyl chloride (DDS) / pyridine / 0.08 h

4: 100 percent / (i-Pr)2NEt / pyridine / 0.01 h

With pyridine; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; hypophosphorous acid; 2,4,5,6-tetramethylbenzenedisulfonyl dichloride; N-ethyl-N,N-diisopropylamine; In pyridine;
DOI:10.1021/jo00381a047