4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride

Base Information

Chemical Name:4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride
CAS No.:87589-30-8
Molecular Formula:C₁₂H₂₁NO₄*ClH
Molecular Weight:279.764
Hs Code.:

Synonyms:4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride

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Chemical Property of 4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride

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Technology Process of 4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride

There total 3 articles about 4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87589-29-5
4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester

: 87589-30-8
4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 0 ℃; for 3h; Yield given;
DOI:10.1021/jm00154a004

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 87589-30-8
4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: 1.) tetrabutylammonium hydrogen sulfate (QHSO₄), 2 M aq. NaOH / 2.) trichloroethylene, reflux, 3 h

3: HCl(g) / ethyl acetate / 3 h / 0 °C

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/jm00154a004

Reference yield:

: 27687-14-5
trans 4-(tert-butyloxycarbonylamino)methylcyclohexanecarboxylic acid

: 87589-30-8
4-Aminomethyl-cyclohexanecarboxylic acid 1-acetoxy-ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) tetrabutylammonium hydrogen sulfate (QHSO₄), 2 M aq. NaOH / 2.) trichloroethylene, reflux, 3 h

2: HCl(g) / ethyl acetate / 3 h / 0 °C

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In ethyl acetate;
DOI:10.1021/jm00154a004