methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl

Base Information

Chemical Name:methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl
CAS No.:1672672-54-6
Molecular Formula:C₁₃H₁₈N₂O₁₀S₂
Molecular Weight:426.425
Hs Code.:

Synonyms:methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl

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Technology Process of methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl

There total 2 articles about methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1618663-81-2
N-(2-hydroxy-1-hydroxymethylethyl)-3-methoxy-4-nitrobenzamide

: 124-63-0
methanesulfonyl chloride

: 1672672-54-6
methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 67579-92-4
3-methoxy-4-nitrobenzoic acid chloride

: 1672672-54-6
methanesulfonic acid 3-methanesulfonyloxy-2-(3-methoxy-4-nitrobenzoylamino)propyl

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 0.25 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane;