9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Base Information

Chemical Name:9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate
CAS No.:913816-02-1
Molecular Formula:C₃₀H₄₀ClN₃O₄
Molecular Weight:542.118
Hs Code.:

Synonyms:9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Suppliers and Price of 9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

There total 6 articles about 9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 9-(4-aminohexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate dihydrochloride

: 74-11-3
para-chlorobenzoic acid

: 913816-02-1
9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Guidance literature:: para-chlorobenzoic acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 1h;

9-(4-aminohexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate dihydrochloride; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 371226-28-7
O-(9-azabicyclo[3.3.1]nonan-3α-yl)-N-(2-methoxy-5-methylphenyl)carbamate

: 913816-02-1
9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃; KI / acetonitrile / Heating

2: hydrazine hydrate / ethanol / 2 h / Heating

3: CH₂Cl₂ / 3 h / 20 °C

With potassium carbonate; hydrazine hydrate; potassium iodide; In ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2006.06.028

Reference yield:

: 1036759-16-6
(2-Methoxy-5-methyl-phenyl)-carbamic acid (1R,3R,5S)-9-[6-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-hexyl]-9-aza-bicyclo[3.3.1]non-3-yl ester

: 913816-02-1
9-(4-(4'-chlorobenzoylamino)hexyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 2 h / Heating

2: CH₂Cl₂ / 3 h / 20 °C

With hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1016/j.bmc.2006.06.028