(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2

Base Information

Chemical Name:(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2
CAS No.:1013399-81-9
Molecular Formula:C₄₈H₇₈B₂S₄Si₇
Molecular Weight:1001.63
Hs Code.:

Synonyms:(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2

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Chemical Property of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2

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Technology Process of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2

There total 1 articles about (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 185910-18-3
1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene

: 78336-55-7
2,2'bi-1,3,2-benzodithiaborole

: 1013399-81-9
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2

Guidance literature:: In benzene; (Ar); soln. of Si compd. and B compd. in C6H6 was freeze-pump-thawed; evacuated; sealed; heated at 60°C for 20 h; opened; solvent removed; chromd. (silica gel, hexane/toluene, 2/1); elem. anal.;
DOI:10.1021/om7008974

Reference yield: 61.0%

: 75-77-4
chloro-trimethyl-silane

: 1013399-81-9
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2

: 1013399-82-0
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe₃)

Guidance literature:: With MeLi; In tetrahydrofuran; diethyl ether; (Ar); soln. of MeLi in Et2O was added to soln. of B compd. in THF at 0°C; stirred at 0°C for 40 min; Me3SiCl was added; solvent removed; chromd. (SiO2 plate, hexane);
DOI:10.1021/om7008974