(2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate

Base Information

Chemical Name:(2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate
CAS No.:1300013-92-6
Molecular Formula:C₂₃H₂₅ClFNO₅
Molecular Weight:449.907
Hs Code.:

Synonyms:(2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate

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Chemical Property of (2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate

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Technology Process of (2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate

There total 2 articles about (2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848194-75-2
o-chlorobenzaldehyde N-(tert-butoxycarbonyl)imine

: 1479-22-7
ethyl 2-fluoro-3-oxo-3-phenylpropionate

: 1300013-92-6
(2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate

: C₂₃H₂₅ClFNO₅

Guidance literature:: With 2BF₄^(1-)*C₄₆H₃₇NOP₂Pd⁽²⁺⁾; In toluene; at 20 ℃; for 7h; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tetlet.2011.02.087

Reference yield:

: 848194-75-2
o-chlorobenzaldehyde N-(tert-butoxycarbonyl)imine

: 1479-22-7
ethyl 2-fluoro-3-oxo-3-phenylpropionate

: (2R,3R)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate

: 1300013-92-6
(2S,3S)-ethyl 2-benzoyl-3-(tert-butoxycarbonylamino)-2-fluoro-3-(2-chlorophenyl)propanoate

Guidance literature:: With C₃₇H₃₁F₆N₃S; In diethyl ether; at 20 ℃; for 24h; optical yield given as %ee; enantioselective reaction;
DOI:10.1055/s-0030-1259319