[Pt(η1-2,2'-biphenyl monoanion)2(COD)]

Base Information

Chemical Name:[Pt(η1-2,2'-biphenyl monoanion)2(COD)]
CAS No.:140673-49-0
Molecular Formula:C₃₂H₃₀Pt
Molecular Weight:609.67
Hs Code.:

Synonyms:[Pt(η1-2,2'-biphenyl monoanion)2(COD)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pt(η1-2,2'-biphenyl monoanion)2(COD)]

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Technology Process of [Pt(η1-2,2'-biphenyl monoanion)2(COD)]

There total 1 articles about [Pt(η1-2,2'-biphenyl monoanion)2(COD)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 12266-72-7
1,5-cyclooctadienediiodoplatinum(II)

: 7732-18-5
water

: 16291-32-0
biphenyl-2,2'-diyl-bis-lithium

: 140673-49-0
[Pt(η1-2,2'-biphenyl monoanion)2(COD)]

Guidance literature:: In diethyl ether; under N2; suspn. of Pt complex in Et2O cooled to -10°C; treated with Li compd. in Et2O; stirred for 2 h; warmed to room temp.; worked up with H2O; aq. phase extd. with CH2Cl2; combined with org. extracts dried over Na2SO4; filtered; solvent evapd. under reduced pressure; recrystd. (toluene-petroleum ether); elem. anal.;
DOI:10.1021/ja030486u