p-Nitrophenyl allenyl ether

Base Information

Chemical Name:p-Nitrophenyl allenyl ether
CAS No.:66397-25-9
Molecular Formula:C₉H₇NO₃
Molecular Weight:177.159
Hs Code.:

Synonyms:p-Nitrophenyl allenyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-Nitrophenyl allenyl ether

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Technology Process of p-Nitrophenyl allenyl ether

There total 7 articles about p-Nitrophenyl allenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 17061-85-7
1-nitro-4-(prop-2-ynyloxy)benzene

: 14146-09-9
2-methyl-5-nitrobenzofuran

: 66397-25-9
p-Nitrophenyl allenyl ether

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; for 0.025h; Product distribution; microwave irradiation; other base, solvent; microwave promoted isomerization of propargyl ethers into allenyl ethers;
DOI:10.1080/00397919708005453

Reference yield: 78.0%

: 17061-85-7
1-nitro-4-(prop-2-ynyloxy)benzene

: 66397-25-9
p-Nitrophenyl allenyl ether

Guidance literature:: With potassium tert-butylate; sodium hydride; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201503598

Reference yield: 75.0%

: 14670-55-4
1,2-dibromo-3-(4-nitrophenyloxy)propane

: 17061-85-7
1-nitro-4-(prop-2-ynyloxy)benzene

: 66397-25-9
p-Nitrophenyl allenyl ether

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; at 60 ℃; for 2h; regioselective reaction;
DOI:10.1055/s-0030-1258813