1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene

Base Information

Chemical Name:1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene
CAS No.:115130-39-7
Molecular Formula:C₆₁H₅₈O₈
Molecular Weight:919.127
Hs Code.:

Synonyms:1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene

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Chemical Property of 1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene

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Technology Process of 1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene

There total 11 articles about 1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 80300-30-7
1-O-acetyl-2,3,4,6-tetra-O-benzyl-D-glucopyranose

: 59434-20-7
1,3,5-tri-O-benzylphloroglucinol

: 115130-39-7
1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; at 0 ℃; for 1h; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c6ob01622g

Reference yield:

: 80300-30-7
1-O-acetyl-2,3,4,6-tetra-O-benzyl-D-glucopyranose

: 59434-20-7
1,3,5-tri-O-benzylphloroglucinol

: 115130-39-7
1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene

: 115130-70-6
2,4,6-tribenzyloxy-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)benzene

Guidance literature:: With triethylsilyl trifluoromethyl sulfonate; In tetrahydrofuran; dichloromethane; at 0 ℃; optical yield given as %de;
DOI:10.1021/ol100315g

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 115130-39-7
1,3,5-tri-O-benzyl-2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) N,N-dimethylformamide, -20 deg. C, 1 h; 2) N,N-dimethylformamide, -20 deg. C, 2h

2: 0.56M diethyl ether *zinc chloride / CH₂Cl₂ / 1 h / Ambient temperature

With sodium hydride; zinc chloride diethyl ether; In dichloromethane;
DOI:10.1016/S0008-6215(00)90879-6