2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane

Base Information

Chemical Name:2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane
CAS No.:112438-31-0
Molecular Formula:C₃₀H₃₈B₂N₂P₂Si₂
Molecular Weight:566.386
Hs Code.:

Synonyms:2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane

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Technology Process of 2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane

There total 4 articles about 2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 112438-36-5
(C₆H₅)2NB(Cl)P{Si(CH₃)3}2

: 59610-41-2
lithium bis(trimethylsilyl)phosphanide-tetrahydrofuran (1/2)

: 112438-31-0
2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane

: 15573-38-3
Tris(trimethylsilyl)phosphane

Guidance literature:: In benzene; byproducts: LiCl; under N2 or Ar or in vac., reflux for 4 h; cooled to room temp., filtered, washed with hexane; elem. anal.;

Reference yield: 47.0%

: 147875-88-5
bis{bis(trimethylsilyl)phosphanyl}(diphenylamino)borane

: 112438-31-0
2,4-bis(diphenylamino)-1,3-bis(trimethylsilyl)-1,3,2,4-diphosphadiboretane

Guidance literature:: In benzene; byproducts: P(Si(CH3)3)3; dissolving corresponding borane (0.5mmol) in benzene (30ml); freezing of soln.; evacuation of flask; refluxing soln. subsequently, 2h;; obtaining a yellow solid and liquid on vacuum evapn. of solvent; remaining compd. by removal of liquid with a cold hexane wash; elem. anal.;;