(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

Base Information

Chemical Name:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride
CAS No.:1279724-06-9
Molecular Formula:C₃₆H₅₈N₈O₂*ClH
Molecular Weight:671.37
Hs Code.:

(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

Synonyms:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

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Chemical Property of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

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Technology Process of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

There total 9 articles about (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279724-22-9
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate

: 1279724-06-9
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

Guidance literature:: With hydrogenchloride; In methanol;
DOI:10.1016/j.bmcl.2010.12.057

Reference yield:

: 217180-77-3
8-azidooctanoyl chloride

: 1279724-06-9
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 1 h / 0 °C

2: N,N-dimethyl-formamide / 48 h

3: copper(II) sulfate; sodium L-ascorbate / ethanol; dichloromethane; water / 20 °C

4: trifluoroacetic acid / dichloromethane / 16 h

5: hydrogenchloride / methanol

With hydrogenchloride; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.057

Reference yield:

: 1248569-13-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

: 1279724-06-9
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(7-(2-amino-1H-imidazol-4-yl)heptyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: copper(II) sulfate; sodium L-ascorbate / ethanol; dichloromethane; water / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 16 h

4.1: hydrogenchloride / methanol

With hydrogenchloride; sodium hydride; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmcl.2010.12.057