N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

Base Information

Chemical Name:N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine
CAS No.:80376-70-1
Molecular Formula:C₁₆H₂₄N₂O₂
Molecular Weight:276.379
Hs Code.:

Synonyms:N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

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Technology Process of N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

There total 2 articles about N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119044-70-1
(E)-N′-tert-butyl-N,N-dimethylformimidamide

: 80376-70-1
N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 89.2 percent / sec-butyllithium / tetrahydrofuran / -78 deg C -> room temperature

2: n-butyllithium / tetrahydrofuran / -78 deg C -> 0 deg C

With n-butyllithium; sec.-butyllithium; In tetrahydrofuran;
DOI:10.1021/ja00367a052

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 80376-66-5
N'-tert-Butyl-N-methyl-N-trimethylsilanylmethyl-formamidine

: 80376-70-1
N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; -78 deg C -> 0 deg C;
DOI:10.1021/ja00367a052

Reference yield:

: 80376-70-1
N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

: 5703-21-9
3,4-dimethoxyphenylacetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; ethanol; H₂O / 6 h / Heating

2: 1.) Cu(OAc)2, 2.) pyridine / 1.) THF, water, reflux, 30 min, 2.) water

With pyridine; copper diacetate; In ethanol; water; acetic acid;
DOI:10.1021/ja00367a052