N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine

Base Information

Chemical Name:N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine
CAS No.:80376-78-9
Molecular Formula:C₁₆H₂₈N₂O₂
Molecular Weight:280.411
Hs Code.:

Synonyms:N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine

Chemical Property:

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Technology Process of N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine

There total 3 articles about N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80376-70-1
N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine

: 80376-78-9
N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; In ethanol; at 0 ℃; for 1h; pH ca.6;
DOI:10.1021/ja00367a052

Reference yield:

: 119044-70-1
(E)-N′-tert-butyl-N,N-dimethylformimidamide

: 80376-78-9
N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 89.2 percent / sec-butyllithium / tetrahydrofuran / -78 deg C -> room temperature

2: n-butyllithium / tetrahydrofuran / -78 deg C -> 0 deg C

3: sodium borohydride, 10percent HCl / aq. ethanol / 1 h / 0 °C / pH ca.6

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; sec.-butyllithium; In tetrahydrofuran; ethanol;
DOI:10.1021/ja00367a052

Reference yield:

: 80376-66-5
N'-tert-Butyl-N-methyl-N-trimethylsilanylmethyl-formamidine

: 80376-78-9
N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / -78 deg C -> 0 deg C

2: sodium borohydride, 10percent HCl / aq. ethanol / 1 h / 0 °C / pH ca.6

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; In tetrahydrofuran; ethanol;
DOI:10.1021/ja00367a052