(2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine

Base Information

Chemical Name:(2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine
CAS No.:175430-93-0
Molecular Formula:C₂₀H₃₄N₂OSi
Molecular Weight:346.588
Hs Code.:

Synonyms:(2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine

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Technology Process of (2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine

There total 3 articles about (2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65651-53-8
(S)-(+)-2-methoxymethyl-1-(1-methylpropylideneamino)pyrrolidine

: 175430-93-0
(2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / LDA / tetrahydrofuran / 1.) 0 deg C, 4 h, 2.) -78 deg C, 1 h; -78 deg C -> room temp.

2: n-BuLi, diisopropylamine / diethyl ether; hexane / 1.) 0 deg C, 4 h; -78 deg C, 0.5 h, 2.) -78 deg C, 1 h; -78 deg C -> room temp.

With n-butyllithium; diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 175430-93-0
(2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / LDA / tetrahydrofuran / 1.) 0 deg C, 4 h, 2.) -78 deg C, 1 h; -78 deg C -> room temp.

2: n-BuLi, diisopropylamine / diethyl ether; hexane / 1.) 0 deg C, 4 h; -78 deg C, 0.5 h, 2.) -78 deg C, 1 h; -78 deg C -> room temp.

With n-butyllithium; diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;

Reference yield:

: 75-03-6
ethyl iodide

: 175430-76-9
(2S)-1-<1'-(Dimethylphenylsilyl)but-2'-ylideneamino>-2-methoxymethylpyrrolidine

: 175430-93-0
(2S,3'S)-1-<3'-(Dimethylphenylsilyl)hex-4'-ylideneamino>-2-methoxymethylpyrrolidine

Guidance literature:: With n-butyllithium; diisopropylamine; In diethyl ether; hexane; Yield given; 1.) 0 deg C, 4 h; -78 deg C, 0.5 h, 2.) -78 deg C, 1 h; -78 deg C -> room temp.;