1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

Base Information

Chemical Name:1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester
CAS No.:211696-87-6
Molecular Formula:C₂₃H₂₁IO₂
Molecular Weight:456.323
Hs Code.:

Synonyms:1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

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Chemical Property of 1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

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Technology Process of 1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

There total 2 articles about 1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 30889-20-4
methyl cyclohexa-2,5-diene-1-carboxylate

: 222421-24-1
(Z)-3-bromo-1-iodo-1,2-diphenylpropene

: 211696-87-6
1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

Guidance literature:: DOI:10.1021/jo981876f

Reference yield:

: 222421-22-9
(Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

: 211696-87-6
1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / CBr₄, PPh₃

2: 60 percent

With carbon tetrabromide; triphenylphosphine;
DOI:10.1021/jo981876f

Reference yield: 80.0%

: 105-53-3
diethyl malonate

: 211696-87-6
1-((E)-3-Iodo-2,3-diphenyl-allyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

: 2-((3aR,5S,7aS)-7a-Methoxycarbonyl-2,3-diphenyl-3a,4,5,7a-tetrahydro-1H-inden-5-yl)-malonic acid diethyl ester

Guidance literature:: With tetrabutyl-ammonium chloride; potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In dimethyl sulfoxide; at 100 ℃; for 23h;
DOI:10.1055/s-1998-1772