(Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

Base Information

Chemical Name:(Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol
CAS No.:222421-22-9
Molecular Formula:C₁₅H₁₃IO
Molecular Weight:336.172
Hs Code.:

Synonyms:(Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

Suppliers and Price of (Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

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Technology Process of (Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

There total 5 articles about (Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 100-58-3
phenylmagnesium bromide

: 222421-22-9
(Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

Guidance literature:: 3-Phenyl-2-propyn-1-ol; phenylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -10 - 20 ℃; Inert atmosphere;

With iodine; In tetrahydrofuran; at -78 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c7ob00499k

Reference yield: 35.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 501-65-5
diphenyl acetylene

: 222421-22-9
(Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

Guidance literature:: diphenyl acetylene; With zirconocene dichloride; ethylmagnesium bromide; In tetrahydrofuran; at 0 ℃; for 3h;

formaldehyd; In tetrahydrofuran; at 50 ℃; for 2h;

With iodine; In tetrahydrofuran; at -78 ℃; for 1h; Further stages.;
DOI:10.1021/jo800232p

Reference yield:

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: phenylmagnesium bromide

: 222421-22-9
(Z)-3-iodo-2-phenyl-3-phenylprop-2-en-1-ol

Guidance literature:: 3-Phenyl-2-propyn-1-ol; phenylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at 0 ℃;

With iodine; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jo0262006