benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate

Base Information

Chemical Name:benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate
CAS No.:781649-92-1
Molecular Formula:C₂₅H₂₉BrN₂O₅
Molecular Weight:517.42
Hs Code.:

Synonyms:benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate

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Chemical Property of benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate

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Technology Process of benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate

There total 2 articles about benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 2-bromo-N-(2,4-dimethoxybenzyl)prop-2-en-1-amine

: 127474-54-8
(R)-2-(benzyloxycarbonylamino)pent-4-enoic acid

: 781649-92-1
benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 18h;
DOI:10.1021/jm070668p

Reference yield:

: 127474-54-8
(R)-2-(benzyloxycarbonylamino)pent-4-enoic acid

: 781649-92-1
benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 18h;

Reference yield: 69.0%

: 781649-92-1
benzyl ((1R)-1-{[(2-bromoprop-2-en-1-yl)(2,4-dimethoxybenzyl)amino]carbonyl}but-3-en-1-yl)carbamate

: 121219-16-7
(2,3-difluorophenyl)boronic acid

: 781650-29-1
benzyl (1R)-1-{[[2-(2,3-difluorophenyl)prop-2-enyl](2,4-dimethoxybenzyl)amino]carbonyl}but-3-enylcarbamate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In water; N,N-dimethyl-formamide; at 75 ℃;
DOI:10.1021/ol8011524