N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine

Base Information

Chemical Name:N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine
CAS No.:157069-78-8
Molecular Formula:C₁₆H₁₄N₂O₂
Molecular Weight:266.299
Hs Code.:

N<sup>1</sup>-(2-vinylbenzoyl)-N<sup>2</sup>-benzoylhydrazine

Synonyms:N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine

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Technology Process of N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine

There total 3 articles about N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 28269-50-3
2-vinylbenzoic acid chloride

: 613-94-5
benzoic acid hydrazide

: 157069-78-8
N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 48h;

Reference yield: 47.0%

: 27326-43-8
2-vinylbenzoic acid

: 613-94-5
benzoic acid hydrazide

: 157069-78-8
N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1021/ol502225p

Reference yield:

: 27326-43-8
2-vinylbenzoic acid

: 157069-78-8
N¹-(2-vinylbenzoyl)-N²-benzoylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Heating

2: 85 percent / Et₃N / CH₂Cl₂ / 48 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane;