C₁₀H₁₀INO

Base Information

• Chemical Name: C₁₀H₁₀INO
• CAS No.: 952429-63-9
• Molecular Formula: C₁₀H₁₀INO
• Molecular Weight: 287.1
• Mol file: 952429-63-9.mol

Synonyms:C₁₀H₁₀INO

Chemical Property of C₁₀H₁₀INO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₀INO

There total 2 articles about C₁₀H₁₀INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

acetamide (60-35-5) + (E)-1,2-diiodostyrene (71022-74-7) → C10H10INO (952429-63-9)

Guidance literature:

With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In toluene; at 40 - 110 ℃; for 21h;

DOI:10.1055/s-2007-983782

Reference yield:

phenylacetylene (536-74-3) → C10H10INO (952429-63-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / I₂ / CH₂Cl₂ / 2.5 h / 20 °C

2: 22 percent / K₂CO₃; N,N'-dimethylethylenediamine; CuI / toluene / 21 h / 40 - 110 °C

With copper(l) iodide; iodine; potassium carbonate; N,N`-dimethylethylenediamine; In dichloromethane; toluene;

DOI:10.1055/s-2007-983782

Reference yield: 93.0%

C10H10INO (952429-63-9) → 2-methyl-5-phenyl-1,3-oxazole (3969-09-3)

Guidance literature:

With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In toluene; at 110 ℃; for 20h;

DOI:10.1055/s-2007-983782

upstream raw materials:

acetamide

(E)-1,2-diiodostyrene

phenylacetylene

Downstream raw materials:

2-methyl-5-phenyl-1,3-oxazole