tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate

Base Information

Chemical Name:tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate
CAS No.:1400565-31-2
Molecular Formula:C₃₃H₅₇N₃O₁₂
Molecular Weight:687.828
Hs Code.:

Synonyms:tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate

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Chemical Property of tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate

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Technology Process of tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate

There total 2 articles about tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 192132-77-7
2-(2-(tert-butoxycarbonylamino)ethoxy)ethyl 4-methylbenzenesulfonate

: 108-73-6
3,5-dihydroxyphenol

: 1400565-31-2
tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate

Guidance literature:: 3,5-dihydroxyphenol; With caesium carbonate; In methanol; at 45 ℃; for 0.5h; Inert atmosphere;

2-(2-(tert-butoxycarbonylamino)ethoxy)ethyl 4-methylbenzenesulfonate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
DOI:10.1055/s-0031-1290444

Reference yield:

: 139115-91-6
2-(2-tert-butyloxycarbonylaminoethoxy)ethanol

: 1400565-31-2
tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: caesium carbonate / methanol / 0.5 h / 45 °C / Inert atmosphere

2.2: 60 °C / Inert atmosphere

With dmap; caesium carbonate; triethylamine; In methanol; dichloromethane;
DOI:10.1055/s-0031-1290444

Reference yield:

: 1400565-31-2
tri-tert-butyl [benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]triscarbamate

: 1400565-37-8
N,N',N''-[benzene-1,3,5-triyltris(oxyethane-2,1-diyloxyethane-2,1-diyl)]tris(4-azido-2,3,5,6-tetrafluorobenzamide)

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C

2: triethylamine / dichloromethane

With triethylamine; In dichloromethane;
DOI:10.1055/s-0031-1290444