5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

Base Information

Chemical Name:5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine
CAS No.:117369-63-8
Molecular Formula:C₁₅H₁₉NO₃
Molecular Weight:261.321
Hs Code.:

Synonyms:5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

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Chemical Property of 5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

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Technology Process of 5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

There total 3 articles about 5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 21572-32-7
2-chloro-1-phenyl-ethanone oxime

: 22141-88-4
3-methoxy-2-methyl-penta-3,4-dien-2-ol

: 117369-63-8
5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

Guidance literature:: With sodium carbonate; In various solvent(s); for 144h; Ambient temperature;

Reference yield: 49.0%

: 22141-88-4
3-methoxy-2-methyl-penta-3,4-dien-2-ol

: 61145-11-7
(1-nitroso-vinyl)-benzene

: 117369-63-8
5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

Guidance literature:: With sodium carbonate; In various solvent(s);

Reference yield:

: 21572-32-7
2-chloro-1-phenyl-ethanone oxime

: 117369-63-8
5,6-Dihydro-6-(1-hydroxy-1-methylethyl)-6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂CO₃ / various solvent(s)

2: 49 percent / Na₂CO₃ / various solvent(s)

With sodium carbonate; In various solvent(s);