(2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester

Base Information

Chemical Name:(2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester
CAS No.:1001431-33-9
Molecular Formula:C₄₉H₆₇Cl₃N₂O₁₁Si₂
Molecular Weight:1022.61
Hs Code.:

(2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester

Synonyms:(2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester

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Chemical Property of (2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester

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Technology Process of (2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester

There total 1 articles about (2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1001431-32-8
(2S,3R)-2-amino-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-pent-4-ynoic acid tert-butyl ester

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1001431-33-9
(2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; at 20 ℃; for 0.583333h;
DOI:10.1002/anie.200702537

Reference yield: 99.0%

: 1001431-33-9
(2S,3R)-3-[2-benzyloxy-5-((1S,2S)-2-benzyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pent-4-ynoic acid tert-butyl ester

: 1001431-34-0
(2S,3R)-3-[5-(1S,2S)-(1-(tert-butyl-dimethylsilanyloxy)-2-carboxy-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-2-hydroxy-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid tert-butyl ester

Guidance literature:: With hydrogen; palladium dihydroxide; In ethyl acetate; at 20 ℃; for 96h; under 760.051 Torr;
DOI:10.1002/anie.200702537