biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate

Base Information

Chemical Name:biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate
CAS No.:1365259-42-2
Molecular Formula:C₂₅H₃₄O₄Si
Molecular Weight:426.628
Hs Code.:

Synonyms:biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate

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Technology Process of biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate

There total 1 articles about biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1336854-05-7
biphenyl-4-ylmethyl (2R,3S)-2,3-dihydroxybutanoate

: 85272-31-7
di-tert-butylsilyl bis(trifluoromethanesulfonate)

: 1365259-42-2
biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 23 ℃; for 30h; Inert atmosphere;
DOI:10.1021/ol300377a

Reference yield: 65.0%

: 1365259-42-2
biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate

: 676-58-4
methylmagnesium chloride

: 3597-91-9
biphenyl-4-yl methanol

: 1365259-43-3
(3R,4S)-4-((di-tert-butyl(methyl)silyl)oxy)-3-hydroxypentan-2-one

: 1365259-44-4
(3R,4S)-4-((di-tert-butyl(methyl)silyl)oxy)-2-methylpentane-2,3-diol

Guidance literature:: biphenyl-4-ylmethyl (4R,5S)-2,2-di-tert-butyl-5-methyl-1,3,2-dioxasilolane-4-carboxylate; methylmagnesium chloride; With N,O-dimethylhydroxylamine*hydrochloride; In tetrahydrofuran; at -10 ℃; for 0.166667h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water; at -10 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol300377a