C₂₇H₂₄N₂O₃

Base Information

Chemical Name:C₂₇H₂₄N₂O₃
CAS No.:1360873-35-3
Molecular Formula:C₂₇H₂₄N₂O₃
Molecular Weight:424.499
Hs Code.:

C<sub>27</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₇H₂₄N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₄N₂O₃

Chemical Property:

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Technology Process of C₂₇H₂₄N₂O₃

There total 1 articles about C₂₇H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1360873-34-2
C₂₅H₂₀N₂O₃

: 74-88-4
methyl iodide

: 1360873-35-3
C₂₇H₂₄N₂O₃

Guidance literature:: C₂₅H₂₀N₂O₃; With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; In tetrahydrofuran; at 50 ℃; for 1h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/anie.201107079

Reference yield:

: 1360873-35-3
C₂₇H₂₄N₂O₃

: 1360873-38-6
C₂₇H₂₅N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydroxylamine hydrochloride / ethanol / 48 h / 20 °C

2: toluene-4-sulfonic acid / ethanol / 48 h / 20 °C

3: mercury dichloride / acetonitrile / 2 h / 80 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; toluene-4-sulfonic acid; mercury dichloride; In ethanol; acetonitrile; 3: Beckmann rearrangement;
DOI:10.1002/anie.201107079

Reference yield:

: 1360873-35-3
C₂₇H₂₄N₂O₃

: C₂₈H₂₇N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; hydroxylamine hydrochloride / ethanol / 48 h / 20 °C

2: toluene-4-sulfonic acid / ethanol / 48 h / 20 °C

3: mercury dichloride / acetonitrile / 2 h / 80 °C / Inert atmosphere

4: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C

With pyridine; hydroxylamine hydrochloride; potassium tert-butylate; toluene-4-sulfonic acid; mercury dichloride; In tetrahydrofuran; ethanol; acetonitrile; 3: Beckmann rearrangement;
DOI:10.1002/anie.201107079