tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)

Base Information

Chemical Name:tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)
CAS No.:26079-98-1
Molecular Formula:C₄₈H₃₃CoN₆O₃
Molecular Weight:800.822
Hs Code.:

tris(1-benzeneazo-naphtholato-<sup>(2)</sup>)-cobalt(III)

Synonyms:tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)

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Chemical Property of tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)

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Technology Process of tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)

There total 3 articles about tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 10534-89-1
hexammine cobalt(III) chloride

: 842-07-9
Sudan I

: 26079-98-1
tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)

Guidance literature:: In ethanol; mixing a small excess of (Coa6)Cl3 with C16H12N2O in 50% ethanol; refluxion for 2 h;; washing with H2O; drying at 80°C;;

Reference yield:

: 71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7
cobalt(II) acetate

: 842-07-9
Sudan I

: 26079-98-1
tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)

Guidance literature:: With dihydrogen peroxide; In ethanol; water; dropwise addn. of 20% aq. H2O2 and a soln. of Co(II)-acetate in 50% alcohol to a soln. of C13H12N2O in hot alcohol; pptn. on storing;;

Reference yield:

: 13859-51-3
pentaaminechlorocobalt(III) dichloride

: 842-07-9
Sudan I

: 26079-98-1
tris(1-benzeneazo-naphtholato-⁽²⁾)-cobalt(III)

Guidance literature:: In ethanol; ammonia; mixing a soln. of C16H12N2O in boiling alcohol with a soln. of (CoCla5)Cl2 in hot dild. aq. NH3; refluxing for 1 h; separation of the ppt. while hot;; repeated treatment with boiling aq. NH3 and boiling alcohol; drying at 100°C;;