ethylmethylphenylsulfonium perchlorate

Base Information

• Chemical Name: ethylmethylphenylsulfonium perchlorate
• CAS No.: 100569-75-3
• Molecular Formula: C₉H₁₃S*ClO₄
• Molecular Weight: 252.719

Synonyms:ethylmethylphenylsulfonium perchlorate

Chemical Property of ethylmethylphenylsulfonium perchlorate

Chemical Property:

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Technology Process of ethylmethylphenylsulfonium perchlorate

There total 1 articles about ethylmethylphenylsulfonium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Ethyl phenyl sulfide (622-38-8) + methyl iodide (74-88-4) → ethylmethylphenylsulfonium perchlorate (100569-75-3)

Guidance literature:

With silver perchlorate; In acetonitrile; for 48h; Ambient temperature;

DOI:10.1246/bcsj.63.2593

Reference yield: 32.0%

methyl 1-indanone-2-carboxylate (22955-77-7) + ethylmethylphenylsulfonium perchlorate (100569-75-3) → methyl 2-methyl-1-oxo-2,3-dihydro-1H-indene-2-carboxylate (72181-95-4) + methyl 2-ethyl-1-oxo-2,3-dihydro-1H-indene-2-carboxylate (100461-75-4) + 1-methoxy-2-(methoxycarbonyl)-1-indene (100461-78-7) + 1-ethoxy-2-(methoxycarbonyl)-1-indene (100461-79-8)

Guidance literature:

With potassium carbonate; In dichloromethane; for 48h; Ambient temperature;

DOI:10.1021/jo00271a025

Reference yield:

ethylmethylphenylsulfonium perchlorate (100569-75-3) + N-methylaniline (100-61-8) → N-methyl-N-ethylaniline (613-97-8) + N,N-dimethyl-aniline (121-69-7,77733-26-7)

Guidance literature:

With potassium carbonate; In dichloromethane; for 72h; Ambient temperature;

DOI:10.1246/bcsj.63.2593

upstream raw materials:

Ethyl phenyl sulfide

methyl iodide

Downstream raw materials:

methyl 2-methyl-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

methyl 2-ethyl-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

1-methoxy-2-(methoxycarbonyl)-1-indene

1-ethoxy-2-(methoxycarbonyl)-1-indene

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