N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate

Base Information

Chemical Name:N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate
CAS No.:112769-41-2
Molecular Formula:C₂₈H₃₂Cl₂N₂O₄S
Molecular Weight:563.545
Hs Code.:

Synonyms:N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate

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Chemical Property of N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate

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Technology Process of N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate

There total 4 articles about N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62827-50-3
thiacyclooctan-3-one 1,1-dioxide

: 112769-41-2
N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / propan-2-ol / 14 h / Heating

2: 1.) conc. HCl, 2.) aq. NaOH / 1.) CH₂Cl₂, 3.5 h, 2.) CH₂Cl₂

With hydrogenchloride; sodium hydroxide; In isopropyl alcohol;
DOI:10.1002/jhet.5570310216

Reference yield:

: 6334-18-5
2,3-dichlorobenzylaldehyde

: 112769-41-2
N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / propan-2-ol / 14 h / Heating

2: 1.) conc. HCl, 2.) aq. NaOH / 1.) CH₂Cl₂, 3.5 h, 2.) CH₂Cl₂

With hydrogenchloride; sodium hydroxide; In isopropyl alcohol;
DOI:10.1002/jhet.5570310216

Reference yield:

: 2-(N-benzyl-N-methyl)aminoethyl 3-aminocrotonate

: 112769-41-2
N-benzyl-N-methylaminoethyl 10-(2,3-dichlorophenyl)-3,4,5,6,7,10-hexahydro-8-methyl-1,1-dioxo-2H-thiacycloocteno<3,2-b>pyridine-9-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / propan-2-ol / 14 h / Heating

2: 1.) conc. HCl, 2.) aq. NaOH / 1.) CH₂Cl₂, 3.5 h, 2.) CH₂Cl₂

With hydrogenchloride; sodium hydroxide; In isopropyl alcohol;
DOI:10.1002/jhet.5570310216