(2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

Base Information

Chemical Name:(2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine
CAS No.:157331-03-8
Molecular Formula:C₂₉H₄₇NO₅
Molecular Weight:489.696
Hs Code.:

Synonyms:(2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

Suppliers and Price of (2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

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Chemical Property of (2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

Chemical Property:

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Technology Process of (2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

There total 6 articles about (2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 693-67-4
bromoundecane

: 157331-03-8
(2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 12 h / 100 °C

2: sodium amide / tetrahydrofuran / 2 h / Heating

3: 59 percent / tetrahydrofuran / 0.17 h / 0 °C

With sodium amide; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)85638-6

Reference yield:

: 60669-22-9
n-undecyltriphenylphosphonium bromide

: 157331-03-8
(2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium amide / tetrahydrofuran / 2 h / Heating

2: 59 percent / tetrahydrofuran / 0.17 h / 0 °C

With sodium amide; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)85638-6

Reference yield:

: 153198-47-1
(2S,3R,6R)-3-benzyloxy-6-hydroxymethyl-1-(methoxycarbonyl)-2-(methoxymethoxy)-methylpiperidine

: 157331-03-8
(2S,3R,6S)-3-benzyloxy-6-<(Z)-1-dodecenyl>-1-(methoxycarbonyl)-2-(methoxymethoxy)methylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl chloride, DMSO; 2.) triethylamine / CH₂Cl₂ / 1.) -78 deg C, 45 min; 2.) rt., 1 h

2: 59 percent / tetrahydrofuran / 0.17 h / 0 °C

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)85638-6