6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine

Base Information

Chemical Name:6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine
CAS No.:197235-40-8
Molecular Formula:C₂₁H₂₁ClN₂O
Molecular Weight:352.864
Hs Code.:

Synonyms:6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine

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Chemical Property of 6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine

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Technology Process of 6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine

There total 3 articles about 6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 6850-57-3
2-methoxybenzylamine

: 197235-38-4
3-bromomethyl-6-chloro-5-methyl-2-phenylpyridine

: 197235-40-8
6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine

Guidance literature:: In ethanol; for 4h; Heating;
DOI:10.1016/S0040-4020(97)00791-6

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 197235-40-8
6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / 12 h / 20 °C

2: 88 percent / toluene / 2 h / 80 °C

3: 85 percent / ethanol / 4 h / Heating

With aluminium trichloride; In ethanol; toluene; 1: Phenylation / 2: Cycloaddition / 3: Substitution;
DOI:10.1016/S0040-4020(97)00791-6

Reference yield:

: 155959-02-7
5-chloro-6-methyl-3-phenyl-2(H)-1,4-oxazin-2-one

: 197235-40-8
6-chloro-N-[(2-methoxyphenyl)methyl]-5-methyl-2-phenyl-3-pyridinemethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / toluene / 2 h / 80 °C

2: 85 percent / ethanol / 4 h / Heating

In ethanol; toluene; 1: Cycloaddition / 2: Substitution;
DOI:10.1016/S0040-4020(97)00791-6