3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester

Base Information

Chemical Name:3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester
CAS No.:200798-74-9
Molecular Formula:C₂₉H₃₃Br₂NO₆
Molecular Weight:651.392
Hs Code.:

Synonyms:3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester

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Chemical Property of 3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester

Chemical Property:

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Technology Process of 3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester

There total 8 articles about 3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53179-78-5,61914-48-5,63538-10-3,63597-73-9,63949-77-9,72691-16-8,72691-18-0,74560-76-2,59952-39-5
3-(2',2'-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylic acid

: 200798-74-9
3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 1 h / Heating

2: 49 percent / 144 h

3: 1.) dicyclohexylcarbodiimide, dimethylaminopyridine / 1.) CH₂Cl₂, 30 min, 2.) CH₂Cl₂, overnight

With dmap; thionyl chloride; dicyclohexyl-carbodiimide;
DOI:10.1021/jf970438r

Reference yield:

: 52918-63-5
deltametrin

: 200798-74-9
3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / 1 M aq. NaOH / tetrahydrofuran / 72 h / Heating

2: SOCl₂ / 1 h / Heating

3: 49 percent / 144 h

4: 1.) dicyclohexylcarbodiimide, dimethylaminopyridine / 1.) CH₂Cl₂, 30 min, 2.) CH₂Cl₂, overnight

With dmap; sodium hydroxide; thionyl chloride; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jf970438r

Reference yield:

: 52315-07-8,65731-83-1,65731-84-2,65732-07-2,66290-20-8,66290-21-9,66841-24-5,67375-30-8,70982-01-3,70982-02-4,71697-59-1,72204-43-4,72204-44-5,83860-31-5,83860-32-6,137430-99-0,137432-55-4
(RS)-α-cyano-3-phenoxybenzyl (1RS,3RS;1RS,3SR)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropane carboxylate

: 200798-74-9
3-(2,2-Dibromo-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid (2-tert-butoxycarbonyl-ethylcarbamoyl)-(3-phenoxy-phenyl)-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1 M aq. NaOH / tetrahydrofuran / 36 h / Heating

2: concd. HCl

3: 49 percent / 144 h

4: 1.) dicyclohexylcarbodiimide, dimethylaminopyridine / 1.) CH₂Cl₂, 30 min, 2.) CH₂Cl₂, overnight

With hydrogenchloride; dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jf970438r