lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)

Base Information

Chemical Name:lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)
CAS No.:405884-52-8
Molecular Formula:C₁₆H₃₂LiO₄*C₂₈H₂₈B
Molecular Weight:670.71
Hs Code.:

Synonyms:lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)

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Chemical Property of lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)

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Technology Process of lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)

There total 1 articles about lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1730-04-7
1,8-diiodonaphthalene

: 436-59-9
dimesitylfluoroborane

: 405884-52-8
lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)

Guidance literature:: With n-butyl lithium; In diethyl ether; hexane; under N2, standard Schlenk techniques; hexane soln. of n-BuLi (2.4 equiv.) added to soln. of 1,8-diiodonaphthalene in Et2O at 0°C; 1 h; soln. of Mes2BF (1.3 equiv.) in Et2O added; warmed to room temp.; stirredovernight; filtered; ppt. washed with Et2O; purified by multiple recrystn. from THF; elem. anal.;
DOI:10.1021/om010946x

Reference yield: 79.0%

: 405884-52-8
lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)

: 32294-60-3
diphenyl ditelluride

: 1258402-67-3
C₃₄H₃₃BTe

Guidance literature:: In diethyl ether; at -20 - 25 ℃;
DOI:10.1038/nchem.838

Reference yield: 79.0%

: 5158-50-9
dimethylboron bromide

: 405884-52-8
lithium dimesityl(1,8-naphthalenediyl)borate tetrakis(tetrahydrofuran)

: 405884-57-3
1-(dimesitylboryl)-8-(dimethylboryl)naphthalene

Guidance literature:: In diethyl ether; under N2, standard Schlenk techniques; 1 equiv. of Me2BBr added to suspn. of Li-B compd. in Et2O; stirred at 25°C for 1 h; filtered; solvent removed by evapn.; recrystd. from pentane; elem. anal.;
DOI:10.1021/om010946x