-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

Base Information

Chemical Name:-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane
CAS No.:159656-91-4
Molecular Formula:C₁₈H₃₃BO₂
Molecular Weight:292.27
Hs Code.:

<S-(4α,5β)>-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

Synonyms:-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

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Chemical Property of -2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

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Technology Process of -2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

There total 1 articles about -2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 69190-62-1
pinacol butylboronate

: 120850-92-2
(1R,2R)-1,2-dicyclohexyl-1,2-ethanediol

: 159656-91-4
-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

Guidance literature:: DOI:10.1002/anie.200453690

Reference yield: 73.0%

: 2146-67-0
(dichloromethyl)lithium

: 159656-91-4
-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

: (4R,5R)-2-((S)-1-Chloro-pentyl)-4,5-dicyclohexyl-[1,3,2]dioxaborolane

Guidance literature:: DOI:10.1002/anie.200453690

Reference yield:

: 75-09-2
dichloromethane

: 159656-91-4
-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane

: C₁₉H₃₄BClO₂

Guidance literature:: dichloromethane; With n-butyllithium; In tetrahydrofuran; at -100 ℃; for 0.5h; Inert atmosphere;

-2-methyl-4,5-dicyclohexyl-1,3,2-dioxaborolane; With zinc(II) chloride; In tetrahydrofuran; at -100 - 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b01432