5,7-bis(benzyloxy)-4,6-dimethylindole

Base Information

Chemical Name:5,7-bis(benzyloxy)-4,6-dimethylindole
CAS No.:99053-75-5
Molecular Formula:C₂₄H₂₃NO₂
Molecular Weight:357.452
Hs Code.:

Synonyms:5,7-bis(benzyloxy)-4,6-dimethylindole

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Chemical Property of 5,7-bis(benzyloxy)-4,6-dimethylindole

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Technology Process of 5,7-bis(benzyloxy)-4,6-dimethylindole

There total 10 articles about 5,7-bis(benzyloxy)-4,6-dimethylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 99053-72-2
3,5-bis(benzyloxy)-2,4-dimethyl-6,β-dinitrostyrene

: 99053-75-5
5,7-bis(benzyloxy)-4,6-dimethylindole

Guidance literature:: With silica gel; iron; acetic acid; In toluene; for 1h; Heating;
DOI:10.1021/ja00311a065

Reference yield:

: 7149-92-0
2,4-dimethoxy-3-methylbenzaldehyde

: 99053-75-5
5,7-bis(benzyloxy)-4,6-dimethylindole

Guidance literature:: Multi-step reaction with 9 steps

1: 89 percent / KOH, NaBH₃CN / methanol / 2.5 h / 25 °C

2: 96 percent / CH₂Cl₂ / 3 h / 25 °C

3: 94 percent / Na, Fe(NO₃)*9H₂O / liquid ammonia / 4 h

4: 58 percent / NBS / benzene / 20 h / 25 °C

5: 86 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 2 h; 2.) 25 deg C, 2 h

6: 78 percent / K₂CO₃, NaI / acetone / 5 h / Heating

7: 77 percent / NH₄OAc / acetic acid / 1.5 h / Heating

8: 48 percent / Cu(NO₃)2*3H₂O / acetic anhydride / 1 h / 65 °C

9: 92 percent / Fe, AcOH, silica gel / toluene / 1 h / Heating

With potassium hydroxide; N-Bromosuccinimide; Fe(NO₃)*9H₂O; ammonium acetate; sodium; silica gel; boron tribromide; iron; sodium cyanoborohydride; potassium carbonate; copper(II) nitrate; acetic acid; sodium iodide; In methanol; dichloromethane; ammonia; acetic anhydride; acetic acid; acetone; toluene; benzene;
DOI:10.1021/ja00311a065

Reference yield:

: 5673-07-4
2,6-dimethoxytoluene

: 99053-75-5
5,7-bis(benzyloxy)-4,6-dimethylindole

Guidance literature:: Multi-step reaction with 10 steps

1: TiCl₄ / CH₂Cl₂ / 1 h / 25 °C

2: 89 percent / KOH, NaBH₃CN / methanol / 2.5 h / 25 °C

3: 96 percent / CH₂Cl₂ / 3 h / 25 °C

4: 94 percent / Na, Fe(NO₃)*9H₂O / liquid ammonia / 4 h

5: 58 percent / NBS / benzene / 20 h / 25 °C

6: 86 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 2 h; 2.) 25 deg C, 2 h

7: 78 percent / K₂CO₃, NaI / acetone / 5 h / Heating

8: 77 percent / NH₄OAc / acetic acid / 1.5 h / Heating

9: 48 percent / Cu(NO₃)2*3H₂O / acetic anhydride / 1 h / 65 °C

10: 92 percent / Fe, AcOH, silica gel / toluene / 1 h / Heating

With potassium hydroxide; N-Bromosuccinimide; Fe(NO₃)*9H₂O; ammonium acetate; sodium; silica gel; boron tribromide; titanium tetrachloride; iron; sodium cyanoborohydride; potassium carbonate; copper(II) nitrate; acetic acid; sodium iodide; In methanol; dichloromethane; ammonia; acetic anhydride; acetic acid; acetone; toluene; benzene;
DOI:10.1021/ja00311a065