C₂₄H₂₇IN₂O₆

Base Information

Chemical Name:C₂₄H₂₇IN₂O₆
CAS No.:1616280-46-6
Molecular Formula:C₂₄H₂₇IN₂O₆
Molecular Weight:566.393
Hs Code.:

C<sub>24</sub>H<sub>27</sub>IN<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₄H₂₇IN₂O₆

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Chemical Property of C₂₄H₂₇IN₂O₆

Chemical Property:

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Technology Process of C₂₄H₂₇IN₂O₆

There total 9 articles about C₂₄H₂₇IN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616280-42-2
methyl 3-{4-[4-amino-2-(1-methyl-5-oxopyrrolidin-2-yl)phenoxy]phenyl}propanoate

: 541-41-3
chloroformic acid ethyl ester

: 1616280-48-8
C₂₄H₂₇IN₂O₆

: 1616280-46-6
C₂₄H₂₇IN₂O₆

Guidance literature:: methyl 3-{4-[4-amino-2-(1-methyl-5-oxopyrrolidin-2-yl)phenoxy]phenyl}propanoate; With hydrogenchloride; potassium iodate; potassium iodide; In 1,4-dioxane; methanol; water; at 50 ℃; for 1.5h;

chloroformic acid ethyl ester; With pyridine; at 0 ℃; for 0.166667h;

Reference yield:

: 1616279-53-8
methyl 4-azido-4-(2-chloro-5-nitrophenyl)butanoate

: 1616280-48-8
C₂₄H₂₇IN₂O₆

: 1616280-46-6
C₂₄H₂₇IN₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 90 °C

1.2: 16 h / 90 °C

2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C

2.2: 1 h / 20 °C

3.1: potassium carbonate / ISOPROPYLAMIDE / 3 h / 120 °C

4.1: ammonium chloride; iron / methanol; tetrahydrofuran; water / 1 h / Reflux

5.1: potassium iodide; potassium iodate; hydrogenchloride / methanol; water; 1,4-dioxane / 1.5 h / 50 °C

5.2: 0.17 h / 0 °C

With hydrogenchloride; potassium iodate; iron; sodium hydride; potassium carbonate; ammonium chloride; triphenylphosphine; potassium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide;

Reference yield:

: 1616279-49-2
ethyl 4-(2-chloro-5-nitrophenyl)-4-[(trimethylsilyl)oxy]butanoate

: 1616280-48-8
C₂₄H₂₇IN₂O₆

: 1616280-46-6
C₂₄H₂₇IN₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 16 h / 20 °C

3.1: diethylazodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine / tetrahydrofuran / 0 - 20 °C

4.1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 90 °C

4.2: 16 h / 90 °C

5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C

5.2: 1 h / 20 °C

6.1: potassium carbonate / ISOPROPYLAMIDE / 3 h / 120 °C

7.1: ammonium chloride; iron / methanol; tetrahydrofuran; water / 1 h / Reflux

8.1: potassium iodide; potassium iodate; hydrogenchloride / methanol; water; 1,4-dioxane / 1.5 h / 50 °C

8.2: 0.17 h / 0 °C

With hydrogenchloride; potassium iodate; diphenyl phosphoryl azide; iron; sodium hydride; potassium carbonate; ammonium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; trifluoroacetic acid; potassium iodide; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide;