3-(4-methoxyphenyl)cyclopentanecarboxaldehyde

Base Information

Chemical Name:3-(4-methoxyphenyl)cyclopentanecarboxaldehyde
CAS No.:190064-52-9
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:3-(4-methoxyphenyl)cyclopentanecarboxaldehyde

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Chemical Property of 3-(4-methoxyphenyl)cyclopentanecarboxaldehyde

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Technology Process of 3-(4-methoxyphenyl)cyclopentanecarboxaldehyde

There total 5 articles about 3-(4-methoxyphenyl)cyclopentanecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 190064-51-8
1-methoxy-4-(3-methoxymethylenecyclopentyl) benzene

: 190064-52-9
3-(4-methoxyphenyl)cyclopentanecarboxaldehyde

Guidance literature:: With perchloric acid; In diethyl ether; at 0 ℃; for 0.25h; Yield given;
DOI:10.1021/jm00122a032

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 190064-52-9
3-(4-methoxyphenyl)cyclopentanecarboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1) a) n-BuLi, b) Cu₂Br₂ / 1) ether, a) hexanes, 0 deg C, 15 min, b) ether, 2) 0 deg C, 1 h

2: 1) t-BuOK / 1) THF, -20 deg C, 15 min, 2) THF, a) -20 deg C, 1 h, b) room temperature, 3 h

3: 70percent aq. HClO₄ / diethyl ether / 0.25 h / 0 °C

With copper(I) bromide; n-butyllithium; perchloric acid; potassium tert-butylate; In diethyl ether;
DOI:10.1021/jm00122a032

Reference yield:

: 930-30-3
cyclopent-2-enone

: 190064-52-9
3-(4-methoxyphenyl)cyclopentanecarboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1) a) n-BuLi, b) Cu₂Br₂ / 1) ether, a) hexanes, 0 deg C, 15 min, b) ether, 2) 0 deg C, 1 h

2: 1) t-BuOK / 1) THF, -20 deg C, 15 min, 2) THF, a) -20 deg C, 1 h, b) room temperature, 3 h

3: 70percent aq. HClO₄ / diethyl ether / 0.25 h / 0 °C

With copper(I) bromide; n-butyllithium; perchloric acid; potassium tert-butylate; In diethyl ether;
DOI:10.1021/jm00122a032