1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal

Base Information

Chemical Name:1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal
CAS No.:148915-87-1
Molecular Formula:C₁₇H₂₆O₃
Molecular Weight:278.392
Hs Code.:

Synonyms:1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal

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Chemical Property of 1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal

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Technology Process of 1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal

There total 4 articles about 1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-30-3
cyclopent-2-enone

: 148915-87-1
1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, 2.) Cu₂Br₂ / 1.) ether, 0 deg C, 30 min, 2.) ether, 0 deg C, 1 h

2: 1.) t-BuOK / 1.) THF, -10 deg C, 20 min, 2.) THF, from -10 deg to RT, 5 h

3: p-toluenesulfonic acid / ethanol / 18 h / Ambient temperature

With copper(I) bromide; n-butyllithium; potassium tert-butylate; toluene-4-sulfonic acid; In ethanol;
DOI:10.1021/ja00064a020

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 148915-87-1
1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, 2.) Cu₂Br₂ / 1.) ether, 0 deg C, 30 min, 2.) ether, 0 deg C, 1 h

2: 1.) t-BuOK / 1.) THF, -10 deg C, 20 min, 2.) THF, from -10 deg to RT, 5 h

3: p-toluenesulfonic acid / ethanol / 18 h / Ambient temperature

With copper(I) bromide; n-butyllithium; potassium tert-butylate; toluene-4-sulfonic acid; In ethanol;
DOI:10.1021/ja00064a020

Reference yield:

: 116526-34-2
3-(4-methoxyphenyl)cyclopentanone

: 148915-87-1
1-formyl-3-(4-methoxyphenyl)cyclopentane diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuOK / 1.) THF, -10 deg C, 20 min, 2.) THF, from -10 deg to RT, 5 h

2: p-toluenesulfonic acid / ethanol / 18 h / Ambient temperature

With potassium tert-butylate; toluene-4-sulfonic acid; In ethanol;
DOI:10.1021/ja00064a020